DMT Crystals

Discussion in 'DIY' started by CaptainFuture, Sep 10, 2012.

  1. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    Its not really difficult, Dear Ones.
    Just cook the bark(100grs per ex) for a day with acidic acid. 3times, discard bark. Cook down to 500ml, let cool. Pour lye in slowly with cooling it, till it gets black.
    Let sit for 24hrs with lid. Pull with 300ml room temp.(!) Naphta(petroleum ether).
    Freeze precip for 24hrs., let dry + scrape, dissolve in max. 35celsius warm Naphta.(use as much Naphta as needed to dissolve all)
    Pour into another bowl, leaving yellow stuff and dirt in the old bowl.
    Cover bowl with saran wrap (foil) and let sit for 2-3 days, xtls will frow slowly. Pour last Naphta residues out and freeze precip the leftover dmt out of it.
    Tada.

    Love, cap
     
  2. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    ok ok .. I went STB , then 3 Sodium Carbonate washes and then did the syran wrap freeze precip first. I need to freeze precip and then do the sryan wrap evap. Got it now. but the only problem is I got shitty bark or ,so I beleive.
     
  3. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    There is no shitty bark :) Maybe cutted heavily with some shit, though you could tell easily by its smell. But red clay soil, who knows.
    Or you are not extracting it right. Stb is def. only for lazy people, I wouldn't recommend it. Cook it down, its almost no work, my advise :)
     
  4. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    and why do the acid part? (not getting shitty) arn't you just going to clean it up in the end. My stuff comes out pretty clean with the super washing soda washes. I'll do a thread sometime in the future with your tek and will see what happens. I'm not getting shitty

    and your telling me not to use more than a 100grams?? I mean shouldn't I use 200gram soo I can atleast expect 2 gram yeild?

    also one more stupid question.. what does this mean? and do NOT divide the residue on the ground of the pot when its cold- its potent. (and will be no problem in the next steps.)
     
    Last edited: Nov 21, 2013
  5. GGTBod

    GGTBod Chronicles of Bodley Administrator Cannabis Doctor Cacti Doctor

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    maybe discard not divide? I stoner stared at that one for a bit like hypnotoad
     
  6. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    good call... I'm going to make a thread in a couple days with my yellow stuff.
     
  7. GGTBod

    GGTBod Chronicles of Bodley Administrator Cannabis Doctor Cacti Doctor

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    You know me mate only done it once and i was a lazy stb whore, smoked those yellow crystals right up too, yes i did papa, soon as i seen anything that looked like glass i was on the scales and onto the crack pipe, i was just about ready to bong the bark i'd waited so long and was so eagerly ignorant and naive i struggled with understanding the concept of 'not orally active' , all i was chasing was the high until i got it and calmed down a bit, took a breath
     
  8. eLShaMukO

    eLShaMukO Moderator Moderator Mushroom Doctor

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    this has picked my interest , its a perfect excuse to buy some new lab tools :D

    the captains makes it sound so easy
     
  9. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    Its damn easy. And much fun to do. Just like the good ol' shroom grow.
    And yes, sorry, meant the divide in a discard way. Meaning- KEEP EVERYTHING you cooked down. Once its basified the solid parts gets liquid again.
    I am working on a 3part 420grs. extraction, so 140grs. each atm, (just for the fun). Which I see as the max, since I was loosing material when cooking it down so low with 200+grs. I mean I cook it down to 300-400mls, which is not much and then I add almost 1:1 cold naphta. That way I get out 80% with the first pull. And quite clean, too. Warm naphta pulls a lot more shit plus it oxidizes the DMT while its in there.

    I am shooting pix of the whole thing, will share tomorrow the first few steps/pix.

    Love, cap
     
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  10. GGTBod

    GGTBod Chronicles of Bodley Administrator Cannabis Doctor Cacti Doctor

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    :popcorn1:

    sunglasses at the ready
     
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  11. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    To lazy :) Will post after first pulls tomorrow.
    Almost got all three jars ready. Just basified the 2nd.
     
  12. Professor PinHead

    Professor PinHead Lost in the Tek.... Administrator Mushroom Doctor Cannabis Doctor Supporter

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  13. elfstone

    elfstone Initiate Mushroom Doctor Supporter

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    What would be the next step to make the fumarate salt?
     
  14. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    Pls read the nexus for the fumarate tek, not doing fum anymore. If I inject the DMT i.m. I just dissolve the freebase xtals in xitric acid water. No need for the fumarate step. Snorting isn't that much fun. (which you might need fum for) In the freezer the freebase is 100% stable, so again no need to do fumarate.

    Btw. here's the promised pictorial review of a recent ex:

    I've put together some pictures of the process of some 420grs mimosa in 3 jars (process done 3 times to get 3 extractions, not one from the whole 420grs!) I've ex'ed 2 weeks ago.

    - Starting with the cooking of the bark 3 times with a ph of 4 reached by adding acetate acid/vinegar essence and then combining and cooking it down to 400ml.
    - Then slowly bit by bit, while stirring/cooling it, basifying it with 25grs. lye/natrium hydroxide.
    - Then pulling it with 200-300ml room temp (!) Naphta/petroleum ether. (that avoids oxidising which I always have (too much for my taste) when using warm Naphta)

    IMG_20131127_151004.jpg IMG_20131127_174453.jpg IMG_20131128_201044.jpg IMG_20131128_201124.jpg IMG_20131128_201824.jpg IMG_20131128_204547.jpg IMG_20131128_204643.jpg IMG_20131128_204804.jpg IMG_20131128_210029.jpg IMG_20131128_210212.jpg IMG_20131130_120435.jpg IMG_20131130_123141.jpg IMG_20131130_123212.jpg IMG_20131130_123716.jpg IMG_20131130_123824.jpg
     
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  15. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    Since all first pulls where a bit dirty (not from oxides but from bark dust and waxes) I dropped them into basified water (some lye up to ph 12) and pulled them all in once with 300ml room temp Naphta. that cleaned them beautifully and I got roughly 3grs. pure shiny (semifluffy) xtals from it which I didn't find needed to be cleaned any further.
    IMG_20131201_094255.jpg IMG_20131201_220734.jpg IMG_20131202_093720.jpg IMG_20131202_093744.jpg IMG_6233.JPG IMG_6235.JPG IMG_6237.JPG IMG_6241.JPG IMG_6240.JPG
     
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  16. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    All other pulls were combined and cleaned with naphta re-xing and grew these xtals with the evaporation method. (the yellow tint is due to me letting it all evape instead of throwing the last rest of naphta out)

    IMG_6243.JPG IMG_6244.JPG IMG_6246.JPG IMG_6247.JPG IMG_6251.JPG IMG_6252.JPG
     
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  17. GGTBod

    GGTBod Chronicles of Bodley Administrator Cannabis Doctor Cacti Doctor

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    I am frothing at the minds eye
     
  18. Weller

    Weller Student of Nature Moderator Cannabis Doctor Cacti Doctor

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    DSCF2392.JPG DSCF2393.JPG DSCF2390.JPG DSCF2475.JPG DSCF2476.JPG I love this thread :super:
    This is a recent re-x on some orange spice.
     
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  19. GGTBod

    GGTBod Chronicles of Bodley Administrator Cannabis Doctor Cacti Doctor

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    :hdrool:

    awesome crystals
     
  20. MB3

    MB3 more fun than a ferret in you

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