DMT Crystals

Discussion in 'DIY' started by CaptainFuture, Sep 10, 2012.

  1. Professor PinHead

    Professor PinHead Lost in the Tek.... Administrator Mushroom Doctor Cannabis Doctor Supporter

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  2. eLShaMukO

    eLShaMukO Moderator Moderator Mushroom Doctor

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    holly shit its incredible
     
  3. rogue

    rogue ♥ Hooked on Mycelium ♥ Moderator Mushroom Doctor Supporter

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    I don't know what I've been waiting for. This seems like the perfect X-mass project :)
    I'll have to give these pages a quick review and then see if my bark is any good still.
     
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  4. CaptainFuture

    CaptainFuture Moderator Moderator Mushroom Doctor

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    Dear Ones,
    just want to share a method how to get out the DMT of Mimosa really fast with only ONE pull with close to zero Oxidation. And then to get out all white pure DMT with a new cleaning method. Honestly don't have the time to read much here myself, so if this is not new, forgive me.

    First I extract the DMT with the following easy and fast AB extraction of 100grs of Mimosa bark shredded:
    - I powderize the bark and use all material
    - Slowly Cooking the bark 3 times, cooking down the combined extraction to roughly 200 to 250mls of liquid (3 times in each 2l of water with 20ml of 5% acetate acid)
    - Cool down and while cooling add 20grs of lye
    - Let sit for a few hours and pull with 350ml of room temp(not warm) Naphta
    - Suck into a glass jar (not bowl, since no need to scrape it later), freeze precipe for 12hours.

    With this method all DMT is pulled with one pull. Along with dust and dirt though. Cooking the extraction down that much ends in a dirty pull, but here comes the new cleaning method into action.

    - I pour off the Naphta and use it later again, its now slightly yellowish, all red dirt is with the DMT sticking to the jar.
    - I pour 300ml water with 15ml 5% acetate acid into the jar and shake. The DMT converts into the acetate salt and the dirt now colorize the water yellowish red.
    - Basify with 20grs of lye
    - Pull the DMT from this with 200ml of Naphta.
    - Naphta comes out very clear and is freeze precipitated in a small glass BOWL.
    - Scraped after 10hours this gives you 99% pure white fluffy DMT. Only a slight yellowish film collects at the bottom of the bowl from oxides(which are not cleaned with this method), if at all.

    You can then surely recrystallize to have thicker crystals if wished.


    Done this with 200grs of whole bark (not powdered bark) and got 2,5grs of pure whitish fluffy DMT.The very thin yellow layer seen in the pix was left behind, you can scrape of the DMT from above that. This yellowish DMT was another 100mgs.

    Pix:

    [​IMG] [​IMG] [​IMG] [​IMG] [​IMG]
     
  5. Weller

    Weller Student of Nature Moderator Cannabis Doctor Cacti Doctor

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    Pretty as a picture :clap:
     
  6. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    i got 200grams left...its powder but i gotta try this....its that freaking all day boil with the vinegar that gets me

    question. why in first step do you use 2L of water with 20ml of vinegar and 2nd step 300ml of water with 15ml of acetate acid(vinegar)?

    just seems like one of those would make the PH to strong or weak? I just wanna make sure I use my last 200grams to the fullest.


    I shouldn't question you... YOU are the MAN. :bow:
     
  7. Rooster

    Rooster Well-Known Member

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    We are all on the same page lmfao. I just put a kilo's worth into the freezer to percipitate. I did Cybs maxion hybrid ab tek. Hope it doesmas good as this looks. I usually just do stb and end up with light yellow spice. Fingers crossed. Peace, Rooster
     
  8. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    three washes with sodium bicarbonate usually helps it get white on the STB
     
  9. Rooster

    Rooster Well-Known Member

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    Where do you get the sodium bicarbonate?
     
  10. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    Last edited: Nov 5, 2014
  11. Rooster

    Rooster Well-Known Member

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    Gotcha. I think I might have some if that. Heres what my spice looks like right now. Just decanted the naptha and put it in front of a fan in my "clean" room. What do you guys think I should do next to keep it white? I know when I scrap it its going to get mixed up and wont be white anymore. Looks like its gonna end up off white/yellowish. By the way this is a 9x13 pyrex. Peace, Rooster image.jpg
     
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  12. Rooster

    Rooster Well-Known Member

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    image.jpg All dry now and it turned yellow as usual. I dont really mind it though. Its very light yellow and I am sure its oretty damn close to pure and was made in a kitchen with mason jars and brownie pans lol. At 10.3g right now. Final weights to come. Peace, Rooster
     
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  13. Rooster

    Rooster Well-Known Member

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    I will try a gram or two for growing crystals later today or tomorrow. Peace, Rooster
     
  14. treewood

    treewood mediocre mycologist Moderator Mushroom Doctor Supporter

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    I'd leave it...but you could re X it... i never do though..... Looks awesome.. like mine.

    soo you got 1%...about what i expect
     
    Last edited: Nov 5, 2014
  15. Rooster

    Rooster Well-Known Member

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    Yep .01% of the pure light yellow crystal and probably around .015% with all the gook from the bottom.
     
  16. Zerky

    Zerky New Member

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    LONG LIVE THIS BEAUTIFUL THREAD!! I actually get a little tearful when looking at the pure artistry of these crystals. I’m only familiar with STB and I’m afraid I have no kitchen options for ALL DAY. I’d be lucky to get 4-6 hours. If there’s anybody out there, do you think that would be enough cool time to get powdered mhrb loose enough to base?
     
  17. Mainframe

    Mainframe Active Member

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    Just picked this up yesterday. I'm am very excited. It will be my first time trying xtal. I'll be sure to get a macro before it all disappears.
    :awetongue:

    Screenshot_20200109-071038.png
     
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